A new class of photocrhomic polymers

F. Stellacci, C. Bertarelli, M.C. Gallazzi and G. Zerbi
 
 Dipartimento Chimica Industriale e Ingegneria Chimica, Politecnico di Milano.

A new family of photochromic molecules (the diarylethene) has been recently developed with excellent optical, termo-chemical and fatigue resistance properties.
These materials become strong candidate for optical data storage and/or other electronic molecular device. Generally these materials are blended with a polymer matrix.
One of the problems with these molecules, still unsolved, is the interaction with the polymer matrix. To solve this problem for the first time a polymer has been synthesized whose repeating unit belongs to the family of diarylethenes. In this way the polymers can be cast as thin film and no blending with a host matrix is required.
The photochromic properties of the polymer are surprisingly better then those of the monomer, its cyclization quantum yield is very high for a photochromic compound being more then twice that of the monomer and is the highest one in the diarylethene family (0.85).
A very important additional property is that the polymer in the conjugated form can be doped with an anodic potential 0.6 V vs. Ag/Ag+, thus opening the field of photoswitchable electronic applications. The optical spectra during cyclisation and opening show a very stable isosbestic point.
The maximum conversion rate (at 313 nm) reachable at the photostationary state is larger then 99%. Vibrational spectra have been investigated and interpreted on the basis of molecular dynamical calculations combined with ab initio calculations (when possible).